Modern Methods for Characterizing Materials and Catalysts

Master and PhD Course

Course description

For a targeted design of materials such as catalysts, functional materials and sensors, a good knowledge of the correlation between structure and function are required. The characterization methods which are available are discussed in this advanced course. The main methods comprise TPR, TPD, chemisorption, thermal gravimetry, IR-, Raman-, TEM, XPS and X-ray diffraction. The methods are presented together with practical examples. Finally, synchrotron methods like X-ray absorption spectroscopy (XAS), X-ray emission (XES) and synchrotron X-ray scattering methods are of strong relevance. In all the functional materials discussed in the course the investigation under reaction conditions is of strong importance to understand their structure in its „working“ state.

 

Wichtige Information / Important note for the Course „Modern Concepts and spectroscopic methods in materials science and catalysis" in Winter Semester WS2023/2024

 

Die Vorlesung wird teilweise in Präsenz, teilweise on-line gehalten. Alle Kursusunterlagen werden über ILIAS bereitsgestellt. Registrieren Sie sich dafür über ILIAS.

This year the course will be conducted in presence. Online participation may be possible (please contact us). Register via ILIAS.

 

Details (in deutsch):

Die Vorlesungsunterlagen sind in Englisch. Wir starten mit einer kurzen Übersicht und einem Vortrag über Raman-Spektroskopie.

Weitere Informationen bei Dmitry Doronkin und Jan-Dierk Grunwaldt).

Dozenten: Dr. Dmitry Doronkin, Prof. Dr. Jan-Dierk Grunwaldt, Dr. Thomas Sheppard, Dr. Anna Zimina und weitere Gäste

Vorlesung: 2 SWS

Ort: HS 006, Geb. 11.21

Zeit: Mittwochs 8.00 Uhr

Vorlesungsmaterialien sind nur für persönlichen Gebrauch.

Details (in English):

The lecture slides are in English. We start with a short overview and a lecture about Raman spectroscopy.

Course lecturers: Dr. Dmitry Doronkin, Prof. Dr. Jan-Dierk Grunwaldt, Dr. Thomas Sheppard, Dr. Anna Zimina and further guests

Course: 2 SWS

Location: HS 006, Geb. 11.21

Official time: Wednesday, 8.00 - 9.00 h

Course material is only for personal use.

 

Letztes Update: 23.10.2023

 

Earlier Course „Modern Concepts and spectroscopic methods in materials science and catalysis", Winter Semester 2018/2019

17.10.2018

- Introduction, Lecturer (Download): Jan-Dierk Grunwaldt

- BET, Chemisorption, (TPR), part I, (Download), Lecturer: Paolo Dolcet

24.10.2018

- Infrared spectroscopy (Download), Lecturer: Dmitry Doronkin

07.11.2018

- BET/Chemisorption + UV-vis spectroscopy (Download), Lecturer: Paolo Dolcet

14.11.2018

- X-ray diffraction (XRD) & introduction to synchrotron radiation (Download), Lecturer: Anna Zimina

21.11.2018

- Small angle X-ray scattering (SAXS), Download, Lecturer: Paolo Dolcet

28.11.2018

- X-ray photoelectron spectroscopy (XPS), Download, Lecturer: Jan-Dierk Grunwaldt

05.12.2018

- Transmission electron microscopy (Download), Guest Lecturer: Di Wang (INT)

12.12.2018

- Thermal analysis, Puls-TA (Download), Lecturer: Maria Casapu

19.12.2018

- Raman spectroscopy (Download), Lecturer: Matthias Stehle

09.01.2019

- X-ray microscopy (XRM) (Download), Lecturer: Thomas Sheppard

16.01.2019

- Introduction to X-ray absorption spectroscopy (XAS) (Download), Lecturer: Anna Zimina

23.01.2019

- X-ray absorption spectroscopy: XANES/EXAFS (Download), Lecturer: Abhijeet Gaur

30.01.2019

- Operando spectroscopy,(Download), Lecturer: Jan-Dierk Grunwaldt

 

 

Course „Modern Concepts and spectroscopic methods in materials science and catalysis", Winter Semester 2017/2018

19.10.2017

- Introduction, Lecturer (Download): Jan-Dierk Grunwaldt

- UV-vis spectroscopy (Download), Lecturer: Thomas Sheppard

26.10.2017

- BET, Chemisorption, TPR (Download), Lecturer: Maria Casapu

02.11.2017

- X-ray photoelectron spectroscopy (XPS) (Download), Lecturer: Jan-Dierk Grunwaldt

09.11.2017

- Raman spectroscopy (Download), Lecturer: Paul Sprenger

16.11.2017

- Infrared spectroscopy (Download), Lecturer: Dmitry Doronkin

23.11.2017

- X-ray diffraction (XRD) (Download), Lecturer: Sabrina Müller, Anna Zimina

30.11.2017

- Transmission electron microscopy (Download), Lecturer: Reinhard Schneider

07.12.2017

- Thermal analysis, Puls-TA, Lecturer: Maria Casapu

14.12.2017

- Introduction to X-ray absorption spectroscopy (XAS) (Download), Lecturer: Anna Zimina

21.12.2017

- X-ray absorption spectroscopy: XANES/EXAFS (Download), Lecturer: Henning Lichtnberg

11.01.2018

- X-ray microscopy (XRM) (Download), Lecturer: Thomas Sheppard

18.01.2018

- Operando spectroscopy, Lecturer: Jan-Dierk Grunwaldt

01.02.2018

- Small angle X-ray scattering (SAXS), Lecturer: Henning Lichtenberg

 

Last update: 18.01.2018

 

To be announced

- Block course, XAS hands-on (1-2 days)

 

Course „Modern Concepts and spectroscopic methods in materials science and catalysis", Winter Semester 2016/2017

 

 

20.10.2016

- Introduction, Lecturer: Henning Lichtenberg (Download); UV-vis spectroscopy, Lecturer: Thomas Sheppard (Download)

 

27.10.2016

- BET, Chemisorption, TPR, Lecturer: Maria Casapu (Download)

 

03.11.2016

- Infrared spectroscopy, Lecturer: Jan-Dierk Grunwaldt (Download)

 

10.11.2016

- Raman spectroscopy, Lecturer: Paul Sprenger (Download)

 

24.11.2016

- Surface analysis (XPS, ISS), Lecturer: Jan-Dierk Grunwaldt (Download)

 

01.12.2016

- X-ray diffraction (XRD) - Theory, In situ spectroscopy, synchrotron radition based, Lecturer: Dmitry Doronkin (Download)

 

08.12.2016

- Thermal analysis, Puls-TA, Lecturer: Maria Casapu (Download)

 

15.12.2016

- Electron microscopy (TEM, STEM, etc.), Guest Lecturer: Di Wang (INT, Download)

 

12.01.2017

- Introduction XAS/ EXAFS, Lecturer: Henning Lichtenberg, Abhijeet Gaur (Download)

 

19.01.2017

- Operando spectroscopy, Lecturer Jan-Dierk Grunwaldt (Download)

 

02.02.2017

- Small angle X-ray scattering (SAXS) and X-ray microscopy (XRM), Lecturer: Henning Lichtenberg, Anna Zimina, Jan-Dierk Grunwaldt, Thomas Sheppard

 

To be announced

- Block course, XAS hands-on (1-2 days)

 

Last update: 05.11.2016

 

 

Course „Modern Concepts and spectroscopic methods in materials science and catalysis", Winter Semester 2015/2016

 

21.10.2015

- Introduction (Download), Lecturer: Henning Lichtenberg ; UV-vis spectroscopy (Download), Lecturer: Thomas Sheppard

28.10.2015

- BET, Chemisorption, TPR (Download), Lecturer: Jan-Dierk Grunwaldt

04.11.2015

- Electron microscopy, energy-disp. X-ray spectroscopy, EELS Part 1 (Download), Lecturer: Reinhard Schneider

11.11.2015

-  Electron microscopy, energy-disp. X-ray spectroscopy, EELS - Part 2, (Download), Lecturer: Reinhard Schneider

18.11.2015

- Infrared spectroscopy (Download), Lecturer: Andreas Gänzler

25.11.2015

- Raman spectroscopy (Download), Lecturer: Paul Sprenger

02.12.2015

- Thermal analysis, Puls-TA (Download), Lecturer: Maria Casapu

09.12.2015

- XRD (Theory, In situ, SR) (Download), Lecturer: Dmitry Doronkin (Anna Zimina)

16.12.2015

- XPS (Download), Lecturer: Ghazal Tofighi, Jan-Dierk Grunwaldt

13.01.2016

- Introduction XAS/ EXAFS (Download), Lecturer: Henning Lichtenberg, Abhijeet Gaur

20.01.2016

- XANES, XES, RIXS (Download), Lecturer: Federico Benzi, Abhijeet Gaur, Henning Lichtenberg

27.01.2016

- SAXS (Download), EPR, NMR (Download), Lecturer: Henning Lichtenberg, Dmitry Doronkin

03.02.2016

- XRM (Download), Lecturer: Sina Baier

10.02.2016

- Operando (Download), Lecturer: Jan-Dierk Grunwaldt

 

Last update: 09.02.2016

 

 

 

 

Schedule of an earlier course in 2014

17.02.2014    Overview, Chemisorption, Surface and Thermal Methods, Electron microscopy

- Short overview (Download, Update 16.02.2014)

- Physisorption (BET), Chemisorption, Temperature programmed methods like TPR
(Download, Update 17.02.2014)

- Electron microscopy, scattering methods, synchrotron radiation sources(download)

- Electron Microscopy and related methods: TEM, SEM, STEM-EDX, in situ electron microscopy

 

18.02.2014  Synchrotron radiation, X-ray microscopy and powder X-ray diffraction

- Synchrotron radiation and synchrotron sources (download)

- X-ray microscopy (download)

- Powder X-ray diffraction

- In situ XRD and synchrotron radiation XRD (download)

19.02.2014    Vibrational methods, UV-vis spectroscopy and surface aalysis

- Infrared spectroscopy (download)

- Raman spectroscopy (download)

- UV-vis spectroscopy (download)

- Surface analysis and X-ray photoelectron spectroscopy

20.02.2014    X-ray absorption spectroscopy and related methods

Preparation: Athena program of the IFFEFIT software (ifeffit-1.2.11), which can be downloaded at http://cars9.uchicago.edu/ifeffit/Downloads.

- Introduction to XAS and EXAFS

- Near edge spectra and X-ray emission: XANES, XES, RIXS

- Block on EXAFS analysis

21.02.2014    Further spectroscopic methods and in situ spectroscopy

- Mößbauer spectroscopy

- EPR spectroscopy

- Thermal analysis, Puls-TA

- In situ studies, in situ cell design and in operando spectroscopy

Final remarks