Moderne Charakterisierungsmethoden für Materialien und Katalysatoren
- Typ: Vorlesung (V)
- Lehrstuhl: KIT-Fakultäten - KIT-Fakultät für Chemie und Biowissenschaften
- Semester: WS 24/25
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Zeit:
Mi. 23.10.2024
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 30.10.2024
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 06.11.2024
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 13.11.2024
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 20.11.2024
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 27.11.2024
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 04.12.2024
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 11.12.2024
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 18.12.2024
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 08.01.2025
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 15.01.2025
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 22.01.2025
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 29.01.2025
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 05.02.2025
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
Mi. 12.02.2025
08:00 - 09:30, wöchentlich
11.21 Seminarraum 006
11.21 Chemische Technik (EG)
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Dozent:
Prof. Dr. Jan-Dierk Grunwaldt
Dr. Thomas Sheppard
Dr. Dmitry Doronkin
Dr. Anna Zimina - SWS: 2
- LVNr.: 5443
- Hinweis: Präsenz/Online gemischt
Zusatzinformationen zu "Moderne Charakterisierungsmethoden für Materialien und Katalysatoren"
Modern Methods for Characterizing Materials and Catalysts
Master and PhD Course
Course description
For a targeted design of materials such as catalysts, functional materials and sensors, a good knowledge of the correlation between structure and function are required. The characterization methods which are available are discussed in this advanced course. The main methods comprise TPR, TPD, chemisorption, thermal gravimetry, IR-, Raman-, TEM, XPS and X-ray diffraction. The methods are presented together with practical examples. Finally, synchrotron methods like X-ray absorption spectroscopy (XAS), X-ray emission (XES) and synchrotron X-ray scattering methods are of strong relevance. In all the functional materials discussed in the course the investigation under reaction conditions is of strong importance to understand their structure in its „working“ state.
Wichtige Information / Important note for the Course „Modern Concepts and spectroscopic methods in materials science and catalysis" in Winter Semester WS2023/2024
Die Vorlesung wird teilweise in Präsenz, teilweise on-line gehalten. Alle Kursusunterlagen werden über ILIAS bereitsgestellt. Registrieren Sie sich dafür über ILIAS.
This year the course will be conducted in presence. Online participation may be possible (please contact us). Register via ILIAS.
Details (in deutsch):
Die Vorlesungsunterlagen sind in Englisch. Wir starten mit einer kurzen Übersicht und einem Vortrag über Raman-Spektroskopie.
Weitere Informationen bei Dmitry Doronkin und Jan-Dierk Grunwaldt).
Dozenten: Dr. Dmitry Doronkin, Prof. Dr. Jan-Dierk Grunwaldt, Dr. Thomas Sheppard, Dr. Anna Zimina und weitere Gäste
Vorlesung: 2 SWS
Ort: HS 006, Geb. 11.21
Zeit: Mittwochs 8.00 Uhr
Vorlesungsmaterialien sind nur für persönlichen Gebrauch.
Details (in English):
The lecture slides are in English. We start with a short overview and a lecture about Raman spectroscopy.
Course lecturers: Dr. Dmitry Doronkin, Prof. Dr. Jan-Dierk Grunwaldt, Dr. Thomas Sheppard, Dr. Anna Zimina and further guests
Course: 2 SWS
Location: HS 006, Geb. 11.21
Official time: Wednesday, 8.00 - 9.00 h
Course material is only for personal use.
Letztes Update: 23.10.2023
Earlier Course „Modern Concepts and spectroscopic methods in materials science and catalysis", Winter Semester 2018/2019
17.10.2018
- Introduction, Lecturer (Download): Jan-Dierk Grunwaldt
- BET, Chemisorption, (TPR), part I, (Download), Lecturer: Paolo Dolcet
24.10.2018
- Infrared spectroscopy (Download), Lecturer: Dmitry Doronkin
07.11.2018
- BET/Chemisorption + UV-vis spectroscopy (Download), Lecturer: Paolo Dolcet
14.11.2018
- X-ray diffraction (XRD) & introduction to synchrotron radiation (Download), Lecturer: Anna Zimina
21.11.2018
- Small angle X-ray scattering (SAXS), Download, Lecturer: Paolo Dolcet
28.11.2018
- X-ray photoelectron spectroscopy (XPS), Download, Lecturer: Jan-Dierk Grunwaldt
05.12.2018
- Transmission electron microscopy (Download), Guest Lecturer: Di Wang (INT)
12.12.2018
- Thermal analysis, Puls-TA (Download), Lecturer: Maria Casapu
19.12.2018
- Raman spectroscopy (Download), Lecturer: Matthias Stehle
09.01.2019
- X-ray microscopy (XRM) (Download), Lecturer: Thomas Sheppard
16.01.2019
- Introduction to X-ray absorption spectroscopy (XAS) (Download), Lecturer: Anna Zimina
23.01.2019
- X-ray absorption spectroscopy: XANES/EXAFS (Download), Lecturer: Abhijeet Gaur
30.01.2019
- Operando spectroscopy,(Download), Lecturer: Jan-Dierk Grunwaldt
Course „Modern Concepts and spectroscopic methods in materials science and catalysis", Winter Semester 2017/2018
19.10.2017
- Introduction, Lecturer (Download): Jan-Dierk Grunwaldt
- UV-vis spectroscopy (Download), Lecturer: Thomas Sheppard
26.10.2017
- BET, Chemisorption, TPR (Download), Lecturer: Maria Casapu
02.11.2017
- X-ray photoelectron spectroscopy (XPS) (Download), Lecturer: Jan-Dierk Grunwaldt
09.11.2017
- Raman spectroscopy (Download), Lecturer: Paul Sprenger
16.11.2017
- Infrared spectroscopy (Download), Lecturer: Dmitry Doronkin
23.11.2017
- X-ray diffraction (XRD) (Download), Lecturer: Sabrina Müller, Anna Zimina
30.11.2017
- Transmission electron microscopy (Download), Lecturer: Reinhard Schneider
07.12.2017
- Thermal analysis, Puls-TA, Lecturer: Maria Casapu
14.12.2017
- Introduction to X-ray absorption spectroscopy (XAS) (Download), Lecturer: Anna Zimina
21.12.2017
- X-ray absorption spectroscopy: XANES/EXAFS (Download), Lecturer: Henning Lichtnberg
11.01.2018
- X-ray microscopy (XRM) (Download), Lecturer: Thomas Sheppard
18.01.2018
- Operando spectroscopy, Lecturer: Jan-Dierk Grunwaldt
01.02.2018
- Small angle X-ray scattering (SAXS), Lecturer: Henning Lichtenberg
Last update: 18.01.2018
To be announced
- Block course, XAS hands-on (1-2 days)
Course „Modern Concepts and spectroscopic methods in materials science and catalysis", Winter Semester 2016/2017
20.10.2016
- Introduction, Lecturer: Henning Lichtenberg (Download); UV-vis spectroscopy, Lecturer: Thomas Sheppard (Download)
27.10.2016
- BET, Chemisorption, TPR, Lecturer: Maria Casapu (Download)
03.11.2016
- Infrared spectroscopy, Lecturer: Jan-Dierk Grunwaldt (Download)
10.11.2016
- Raman spectroscopy, Lecturer: Paul Sprenger (Download)
24.11.2016
- Surface analysis (XPS, ISS), Lecturer: Jan-Dierk Grunwaldt (Download)
01.12.2016
- X-ray diffraction (XRD) - Theory, In situ spectroscopy, synchrotron radition based, Lecturer: Dmitry Doronkin (Download)
08.12.2016
- Thermal analysis, Puls-TA, Lecturer: Maria Casapu (Download)
15.12.2016
- Electron microscopy (TEM, STEM, etc.), Guest Lecturer: Di Wang (INT, Download)
12.01.2017
- Introduction XAS/ EXAFS, Lecturer: Henning Lichtenberg, Abhijeet Gaur (Download)
19.01.2017
- Operando spectroscopy, Lecturer Jan-Dierk Grunwaldt (Download)
02.02.2017
- Small angle X-ray scattering (SAXS) and X-ray microscopy (XRM), Lecturer: Henning Lichtenberg, Anna Zimina, Jan-Dierk Grunwaldt, Thomas Sheppard
To be announced
- Block course, XAS hands-on (1-2 days)
Last update: 05.11.2016
Course „Modern Concepts and spectroscopic methods in materials science and catalysis", Winter Semester 2015/2016
21.10.2015
- Introduction (Download), Lecturer: Henning Lichtenberg ; UV-vis spectroscopy (Download), Lecturer: Thomas Sheppard
28.10.2015
- BET, Chemisorption, TPR (Download), Lecturer: Jan-Dierk Grunwaldt
04.11.2015
- Electron microscopy, energy-disp. X-ray spectroscopy, EELS Part 1 (Download), Lecturer: Reinhard Schneider
11.11.2015
- Electron microscopy, energy-disp. X-ray spectroscopy, EELS - Part 2, (Download), Lecturer: Reinhard Schneider
18.11.2015
- Infrared spectroscopy (Download), Lecturer: Andreas Gänzler
25.11.2015
- Raman spectroscopy (Download), Lecturer: Paul Sprenger
02.12.2015
- Thermal analysis, Puls-TA (Download), Lecturer: Maria Casapu
09.12.2015
- XRD (Theory, In situ, SR) (Download), Lecturer: Dmitry Doronkin (Anna Zimina)
16.12.2015
- XPS (Download), Lecturer: Ghazal Tofighi, Jan-Dierk Grunwaldt
13.01.2016
- Introduction XAS/ EXAFS (Download), Lecturer: Henning Lichtenberg, Abhijeet Gaur
20.01.2016
- XANES, XES, RIXS (Download), Lecturer: Federico Benzi, Abhijeet Gaur, Henning Lichtenberg
27.01.2016
- SAXS (Download), EPR, NMR (Download), Lecturer: Henning Lichtenberg, Dmitry Doronkin
03.02.2016
- XRM (Download), Lecturer: Sina Baier
10.02.2016
- Operando (Download), Lecturer: Jan-Dierk Grunwaldt
Last update: 09.02.2016
Schedule of an earlier course in 2014
17.02.2014 Overview, Chemisorption, Surface and Thermal Methods, Electron microscopy
- Short overview (Download, Update 16.02.2014)
- Physisorption (BET), Chemisorption, Temperature programmed methods like TPR
(Download, Update 17.02.2014)
- Electron microscopy, scattering methods, synchrotron radiation sources(download)
- Electron Microscopy and related methods: TEM, SEM, STEM-EDX, in situ electron microscopy
18.02.2014 Synchrotron radiation, X-ray microscopy and powder X-ray diffraction
- Synchrotron radiation and synchrotron sources (download)
- X-ray microscopy (download)
- Powder X-ray diffraction
- In situ XRD and synchrotron radiation XRD (download)
19.02.2014 Vibrational methods, UV-vis spectroscopy and surface aalysis
- Infrared spectroscopy (download)
- Raman spectroscopy (download)
- UV-vis spectroscopy (download)
- Surface analysis and X-ray photoelectron spectroscopy
20.02.2014 X-ray absorption spectroscopy and related methods
Preparation: Athena program of the IFFEFIT software (ifeffit-1.2.11), which can be downloaded at http://cars9.uchicago.edu/ifeffit/Downloads.
- Introduction to XAS and EXAFS
- Near edge spectra and X-ray emission: XANES, XES, RIXS
- Block on EXAFS analysis
21.02.2014 Further spectroscopic methods and in situ spectroscopy
- Mößbauer spectroscopy
- EPR spectroscopy
- Thermal analysis, Puls-TA
- In situ studies, in situ cell design and in operando spectroscopy
Final remarks